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An oscillatory ball mill Mixer Mill MM301, Retsch Co., Germany was used for cryo milling as follows 1 g of indomethacin was placed into a 25 mL milling jar and milled with two 12 mm balls for 120 minutes. The jars were immersed in liquid nitrogen for 3 min before milling and repeatedly for 3 min at 15 min intervals. Read More
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We have oscillatory ball mill mixermill mm301 retsch,Themixer millMM 400 is a compact versatile bench-top unit, which has been developed specially for dry, wet and cryogenic grinding of small amounts of sample. It can mix and homogenize powders and suspensions in only a few seconds. It is also perfectly suitable for the disruption of biological cells as well as for DNA/RNA and protein extraction.
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2.2.1. Sample preparation by ball milling (cold room) The drugs were milled using an oscillatory ball mill (Mixer Mill MM301, Retsch amp Co., Germany). A central composite face centered design was used for the milling experiments for both compounds. The experimental design was created using MODDE software (version 7, Umetrics AB, Sweden).
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