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Ball milling and particle size analyses of metakaolin Using a planetary high-energy ball mill (Retsch PM 400), the metakaolin samples were ball milled for 1, 2, 3 hours at rotation speeds of Ω = 400 rpm for the disc and ω = 800 rpm for the vials respec-tively. A particle size distribution test was carried

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into fine powders using a rapid ball mill (MGS Sarl) with a porcelain jar and microspheres of high-grade alumina as a grinding medium. The obtained powders of kaolin (Dib 0) were calcined in a programmable elec-tric furnace (MGS Sarl) for 4 h at a heating and cooling rate of 5 °C/min at 700 °C to obtain metakaolin (MK-Dib 0). It is important ...

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